Experimental Evaluation of Procedures for Heat Capacity Measurement by Differential Scanning Calorimetry

Experimental evaluation of the procedures adopted for heat capacity measurements employing differential scanning calorimetry (DSC) has been carried out by taking nickel and sapphire as test samples. Among the various methodologies reported in literature, the absolute dual step method was chosen for this purpose due to its simplicity and minimum number of measurements required. By proper temperature and heat flux calibration employing indium as reference, it was possible to obtain the calibration factor independent of temperature. This was ascertained by analysing other pure metals namely Sn, Zn, Cd, and Pb and determining their melting temperatures and heats of melting. Various operator- and sample-dependent parameters such as heating rate, sample mass, the structure of the sample, reproducibility and repeatability in the measurements were investigated. Heat capacities of both nickel and sapphire have been determined using the above method. Further, the heat capacity of nickel has also been determined using the widely employed three-step method taking sapphire as the heat flux calibration standard. Both methods yielded the comparable heat capacity values for nickel. Based on the parameters investigated and their influence, it could be concluded that reasonably precise and accurate heat capacity measurements are possible with DSC. One advantage of this method is the elimination of a separate calibration run using a reference material of known heat capacity. This revised version was published online in August 2006 with corrections to the Cover Date.     

HLS注入段束流位置探头定标电场的拟合和误差计算

 描述了束流位置探测器(BPM)探头定标、定标电场的拟合和误差计算。该定标系统采用了具有调节精度为10μm垂直放置真空管道的天线模拟定标装置和分辨率高达1μm外差式、窄带频域信号处理电子学线路。并推导出针对合肥光源（HLS）定标系统条件下的电场拟合函数及相关的BPM-Mapping图和误差计算结果,较精确地计算出该高精度定标系统误差。     

迷宫密封湍流增阻的数值研究

迷宫密封是依靠节流间隙中的节流过程和迷宫空腔内的动能耗散过程来实现密封的,这两个流体流动过程从本质上规定了迷宫密封的密封性能。通过密封内部流动本质的研究,合理利用湍流流动的规律和特点,能够发挥密封内部湍流的增阻作用,提高密封性能。本文数值计算了一种锯齿型径向迷宫密封的内部流动,得到了密封内部的流动形态,揭示了密封内部流动与密封性能的关系。结果表示,密封存在一个最佳的齿插入长度。在最佳齿插入长度时,尽管节流间隙较大,但由于节流间隙内流动收缩和偏转,间隙的有效通流面积却很小,泄漏介质可以在间隙中获得较大的速度,在迷宫空腔内形成正确的耗散涡流,密封具有最佳的密封效果。所以,充分发挥湍流增阻的作用,可以突破节流间隙的微小尺寸限制,实现较大间隙下的良好密封。这不仅会给迷官密封的制造、安装及运行等带来很大的方便,而且可以为发展新的迷宫密封技术奠定理论基础。     

Effect of Pump Bandwidth: Enhancement of Output Intensity Noise Squeezing in Raman Lasers

The effect of the pump bandwidth on the quantum statistical properties of Raman lasers is investigated. It is shown that the pump bandwidth may lead to the enhancement of output intensity noise squeezing even though it reduces the Mandel Q parameter.     

磁性液体对射流冲击传热的强化

本文对磁液应用于射流冲击传热的影响进行了实验研究。采用变压器油和煤油基磁液ＣＩ－２０Ｂ作为工质,把 １３×５ ｍｍ的康铜金属膜作为加热面和传热面,进行自由表面液体窄缝射流冲击,使用的喷嘴窄缝宽度为 ２５０微米,射流速度变化范围 ５．７ ｍ／ｓ～８．５ ｍ／ｓ。分别对附加磁液前后的射流传热实验结果进行比较,表明磁液的使用对射流冲击传热具有一定的强化。     

多孔涂层横向抽吸效应强化膜状凝结换热的研究

研究多孔涂层界面抽吸效应对强化膜状凝结换热的影响。考察了多孔涂层的特性参数对凝液膜厚度和换热系数的影响。与Nusselt理论预示值对照表明,多孔涂层界面抽吸效应是强化膜状凝结换热的重要因素。     

光纤干涉测距中的量程倍增系统

利用光纤传感技术,实现了一种可以测量１ｍ以上的绝对距离的光纤干涉测距的倍增系统。它主要采用两个干涉仪,分别对靶标进行定位及对光程进行调谐和对距离进行测量,通过引入已精确标定的光纤,利用短导轨,实现了高精度、大距离的测量。     

合成近场校准基阵的方法研究

本文利用单根的束控线阵来构造一个虚拟近场校准基阵,使换能器能在它的近场直接测量辐射声场特性。通过利用改进的矩阵稳定技术,解决了求解束控线阵的束控系数时最小二乘解的稳定性和实用性问题。借助计算机仿真,研究了特定线阵条件下,合成近场测量基阵（Ｓ－ＮＦＣＡ）的近场空间的平面波均匀性与线阵间的间距、线阵的工作频率之间的关系。并以小球源为阵元合成一虚拟平面ＮＦＣＡ,用它对一平面喇叭换能器的近场测量得到远场指向性,并与远场实测结果比较,得到了相当吻合的结果。     

最小相关系数的多元校正波长选择算法

在近红外光谱的定量分析中,由于仪器的精密程度越来越高,采集的光谱数据通常具有很高的维度.因此,波长选择对于剔除噪声及冗余变量,简化模型,提高模型的预测性能是必不可少的.近红外光谱特征波长选择方法众多,但变量间的多重共线性问题仍是导致模型效果较差的一个关键问题.变量间共线性可以通过相关系数进行分析,当相关系数高于0.8,...     

用查找表搜索匹配方法标定CRT

传统的查找表法在标定ＣＲＴ 时,假定ＣＲＴ 单枪作用时所显示颜色的色品坐标恒定不变,而实际上却有较大变化,对标定的精度有较大的影响。因此提出用一种三维搜索匹配方法对查找表法进行改进,提高了ＣＲＴ 的标定精度。